Genes and proteins expressed specifically in testis


 

Principal Investigator : Anil K Suri

Project Associates/Assistants
Shalini Sen
Anuradha Balan (till Jan 2001)
Nirmala Jagdish (till Sep 2000)
P John Leema Rose (since Dec 2000)
Maitreyi Rajala (since Aug 2000)
A C Shymala (since Jul 2000)
Shikha Yadav (since Dec 2000)

Collaborator
John C Herr, Univ of Virginia, USA

Morphological and biochemical observations along the molecular biological approaches suggest that germ cell differentiation is accompanied by selective gene expression. However, the molecular mechanisms regulating the cell type specific gene expression during spermatogenesis are yet to be determined. Identification of testis specific genes and their characterization would thus enhance our understanding about the functioning of sperm at the molecular level. This would possibly highlight the mechanism of sperm development, maturation and sperm-egg interaction. This project’s goal is to investigate testis specific genes expressed in a restricted, temporal and spatial manner during spermatogenesis.

Cloning, expression and purification of hss recombinant protein

The human sperm surface recombinant protein hss construct A (complete ORF having Leucine zipper LZ, antgenic determinant sites A1-A3, Transmembrane domain T and cytosolic domain C), construct C (LZ, A1-A3, DT, DC), and construct D (A1-A3, DLZ, DT, DC) were cloned in pET 28b (+) and successfully expressed in E.coli BL 21 (DE3) pLyse. The recombinant protein was subjected to a purification procedure. Since the recombinant protein was fused with 6 Histidine residue of the expression vector at COOH terminus, the expressed protein was purified using Ni-Histidine bind resin affinity chromatography. Initially small-scale purification of recombinant protein was done by His- Bind resin using two approaches: pH gradient and by eluting with imidazole. It was observed that the recovery of recombinant protein was higher using imidazole as compared to pH gradient. Therefore 1 M Imidazole was used for large-scale purification of recombinant protein.

Before initiating further studies with hss recombinant protein, recombinant protein was subjected to mass spectrometry in order to find whether our recombinant expressed protein had the same hss deduced sequence which we have published (EMBL Acc. No. X91879). The recombinant protein was run on SDS page gel and band of interest was processed. The gel piece was transferred to a siliconized tube and washed and destained in 200 ml 50% methanol overnight. The gel pieces were treated in 20 ng/ml trypsin in 50 mM ammonium bicarbonate on ice for 10 min. Any excess trypsin solution was removed and 20 ml 50 mM ammonium bicarbonate added. The sample was digested over night at 37°C and the peptides formed extracted from polyacrylamide in 30 ml aliquots of 50% acetonitrle/5% formic acid. These extracts were combined and evaporated to 25 ml for LC-MS analysis. The data thus generated were analyzed by database searching using the Sequest search algorithm. Results of the Mass Spectrometry revealed that micro-sequencing of hss recombinant protein (approximately 45% of recombinant protein was analyzed of various peptide lengths: in total 205 amino acids analyzed of deduced 766 amino acids) matched with our deduced protein which we have cloned. No other protein was found to have homology with our protein, therefore it is a novel protein.

The hss recombinant protein was used to immunize rabbits, rats and monkeys. Antibodies thus raised against recombinant protein are being used to examine the properties of antibodies to investigate the affect on sperm functioning using several functional in vitro assays.

Genomic structural organization and chromosomal mapping of hss gene

We have cloned a human sperm surface gene designated as hss gene, which encodes for a protein having Leuzine zipper (LZ), antigenic determinant sites (A1-A3), transmembrane domain (T) and cytosolic domain (C). Tissue distribution of hss gene was studied using different tissue mRNA that revealed that hss gene was exclusively expressed in testis only. Expression of hss transcript was observed only in round spermatids indicating post meiotic haploid gene expression. Human genomic leucocytic library was screened using hss cDNA. Genomic clone was successfully isolated and was sequenced. Attempts were made to do the chromosomal mapping of hss gene. Fluorescent in situ hybridization to normal human male metephase chromosome was carried out. Assessment of well spread metaphase chromosomes indicated signals of hss gene on both homologous chromosome 17, mapping long arm of chromosome 17 at band 17q 21.3-q 22.

Studies on post-transcriptional regulation of human hss gene during spermatogenesis

The hss nucleotide sequence revealed the presence of three unique palindromic motifs and hairpin loop in 5’ and 3’ sequence. It is observed that Pal I is present in 5’ UTR, Pal II is present just before stop codon in ORF and Pal III is present in 3’ UTR. It was earlier reported that using in vitro synthesized mRNA transcript of respective Palindromic motifs, specific RNA protein complexes were formed using testicular cytosolic extract. Further on Northwestern studies have been carried out to find out the mass of those RNA binding proteins, which bind specifically to these motifs. Attempts are also being made to screen the testis cDNA expression library to fish out the clone of interest, which expresses the RNA binding protein, specifically binding to these motifs.